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Rh(III)-Catalyzed Allylic C(sp(3))–H Activation of Alkenyl Sulfonamides: Unexpected Formation of Azabicycles()

Herein we report that unsaturated N-sulfonamides undergo a Rh(III)-catalyzed allylic C(sp(3))-H activation followed by insertion with an exogenous internal alkyne. The reaction generates [3.3.0], [4.3.0] and [5.3.0] azabicyclic structures with excellent diastereoselectivity. Deuterium-labeling exper...

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Detalhes bibliográficos
Publicado no:Angew Chem Int Ed Engl
Main Authors: Archambeau, Alexis, Rovis, Tomislav
Formato: Artigo
Idioma:Inglês
Publicado em: 2015
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4676418/
https://ncbi.nlm.nih.gov/pubmed/26358769
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201504150
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