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Synthesis of cholesteryl-α-D-lactoside via generation and trapping of a stable β-lactosyl iodide

The generation of β-lactosyl iodide was carried out under non-in situ-anomerization, metal free conditions by reacting commercially available β-per-O-acetylated lactose with trimethylsilyl iodide (TMSI). The β-iodide was surprisingly stable as evidenced by NMR spectroscopy. Introduction of octanol o...

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Vydáno v:Tetrahedron Lett
Hlavní autoři: Davis, Ryan A., Fettinger, James C., Gervay-Hague, Jacquelyn
Médium: Artigo
Jazyk:Inglês
Vydáno: 2015
Témata:
On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC4629507/
https://ncbi.nlm.nih.gov/pubmed/26543257
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2015.05.012
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