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Synthesis of cholesteryl-α-D-lactoside via generation and trapping of a stable β-lactosyl iodide
The generation of β-lactosyl iodide was carried out under non-in situ-anomerization, metal free conditions by reacting commercially available β-per-O-acetylated lactose with trimethylsilyl iodide (TMSI). The β-iodide was surprisingly stable as evidenced by NMR spectroscopy. Introduction of octanol o...
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| Publicado en: | Tetrahedron Lett |
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| Autores principales: | , , |
| Formato: | Artigo |
| Lenguaje: | Inglês |
| Publicado: |
2015
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| Materias: | |
| Acceso en línea: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4629507/ https://ncbi.nlm.nih.gov/pubmed/26543257 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2015.05.012 |
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