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Triphosgene–Amine Base Promoted Chlorination of Unactivated Aliphatic Alcohols

Unactivated α-branched primary and secondary aliphatic alcohols have been successfully transformed into their corresponding alkyl chlorides in high yields upon treatment with a mixture of triphosgene and pyridine in dichloromethane at reflux. These mild chlorination conditions are high yielding, ste...

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Detalhes bibliográficos
Main Authors: Villalpando, Andrés, Ayala, Caitlan E., Watson, Christopher B., Kartika, Rendy
Formato: Artigo
Idioma:Inglês
Publicado em: 2013
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4153350/
https://ncbi.nlm.nih.gov/pubmed/23496045
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo400341n
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