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Preparation and Purification of Zinc Sulphinate Reagents for Organic Synthesis

The present protocol details the synthesis of zinc bis(alkanesulphinate)s that can be used as general reagents for the formation of radical species. The zinc sulphinates described herein have been generated from the corresponding sulphonyl chlorides by treatment with zinc dust. The products may be u...

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Bibliografiska uppgifter
Huvudupphovsmän: O’Hara, Fionn, Baxter, Ryan D., O’Brien, Alexander G., Collins, Michael R., Dixon, Janice A., Fujiwara, Yuta, Ishihara, Yoshihiro, Baran, Phil S.
Materialtyp: Artigo
Språk:Inglês
Publicerad: 2013
Ämnen:
Länkar:https://ncbi.nlm.nih.gov/pmc/articles/PMC4114315/
https://ncbi.nlm.nih.gov/pubmed/23640168
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1038/nprot.2013.059
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