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Preparation and Purification of Zinc Sulphinate Reagents for Organic Synthesis

The present protocol details the synthesis of zinc bis(alkanesulphinate)s that can be used as general reagents for the formation of radical species. The zinc sulphinates described herein have been generated from the corresponding sulphonyl chlorides by treatment with zinc dust. The products may be u...

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Detalhes bibliográficos
Main Authors: O’Hara, Fionn, Baxter, Ryan D., O’Brien, Alexander G., Collins, Michael R., Dixon, Janice A., Fujiwara, Yuta, Ishihara, Yoshihiro, Baran, Phil S.
Formato: Artigo
Idioma:Inglês
Publicado em: 2013
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4114315/
https://ncbi.nlm.nih.gov/pubmed/23640168
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1038/nprot.2013.059
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