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A Practical Synthesis and X-ray Crystallographic Analysis of Dithymoquinone, a Photodimer of Thymoquinone

An updated and practical approach to the synthesis of dithymoquinone via one-step photoirradiation of thymoquinone (2-methyl-5-isopropyl-1,4-benzoquinone) is described. Synthesis resulted in a 55% yield of one structural isomer (trans-anti derivative), as confirmed by HPLC, NMR spectroscopy and firs...

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Main Authors: Myers, Alan L., Zhang, Yan-Ping, Kramer, Mark A., Bornmann, William G., Kaseb, Ahmed, Yang, Peiying, Tran, Hai T.
Formato: Artigo
Idioma:Inglês
Publicado: 2012
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Acceso en liña:https://ncbi.nlm.nih.gov/pmc/articles/PMC4039186/
https://ncbi.nlm.nih.gov/pubmed/24883052
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.2174/157017812803901890
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