Long-Observation-Window Band-Selective Homonuclear Decoupling: Increased Sensitivity and Resolution in Solid-State NMR Spectroscopy of Proteins

Sensitivity and resolution are the two fundamental obstacles to extending solid-state nuclear magnetic resonance to even larger protein systems. Here, a novel long-observation-window band-selective homonuclear decoupling (LOW BASHD) scheme is introduced that increases resolution up to a factor of 3...

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Main Authors: Struppe, Jochem O., Yang, Chen, Wang, Yachong, Hernandez, Roy V., Shamansky, Lisa M., Mueller, Leonard J.
Format: Artigo
Sprog:Inglês
Udgivet: 2013
Fag:
Article
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC4017862/
https://ncbi.nlm.nih.gov/pubmed/24095840
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jmr.2013.09.001
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