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A NMR Experiment for Simultaneous Correlations of Valine and Leucine/Isoleucine Methyls with Carbonyl Chemical Shifts in Proteins

A methyl-detected ‘out-and-back’ NMR experiment for obtaining simultaneous correlations of methyl resonances of Valine and Isoleucine/Leucine residues with backbone carbonyl chemical shifts, SIM-HMCM(CGCBCA)CO, is described. The developed pulse-scheme serves the purpose of convenience in recording a...

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Bibliografiske detaljer
Main Authors: Tugarinov, Vitali, Venditti, Vincenzo, Clore, G. Marius
Format: Artigo
Sprog:Inglês
Udgivet: 2013
Fag:
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC3974575/
https://ncbi.nlm.nih.gov/pubmed/24346684
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-013-9803-1
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