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Isolation of a 2-Hydroxytetrahydrofuran Complex from Copper-Promoted Hydroxylation of THF

A complex of a binucleating macrocyclic ligand comprising a [Cu(II)(μ-OH)Na](2+) core reacts with CuI in THF/CH(3)CN to yield a novel species with a deprotonated 2-hydroxytetrahydrofuran (THF-2-ol) bridging between Cu(II) and Na(I) ions. The complexes were characterized by X-ray crystallography, EPR...

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Detalhes bibliográficos
Main Authors: Halvagar, Mohammad Reza, Tolman, William B.
Formato: Artigo
Idioma:Inglês
Publicado em: 2013
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3799914/
https://ncbi.nlm.nih.gov/pubmed/23886308
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ic401446s
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