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Minimizing the Amount of Nitromethane in Palladium Catalyzed Cross Coupling with Aryl Halides

A method for the formation of arylnitromethanes is described that employs readily available aryl halides or triflates and small amounts of nitromethane in a dioxane solvent, thereby reducing the hazards associated with this reagent. Specifically, 2–10 equivalents (1–5% v/v) of nitromethane can be em...

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Autors principals: Walvoord, Ryan R., Kozlowski, Marisa C.
Format: Artigo
Idioma:Inglês
Publicat: 2013
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Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC3778657/
https://ncbi.nlm.nih.gov/pubmed/23895411
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo401249y
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