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Identifying Inter-Residue Resonances in Crowded 2D (13)C-(13)C Chemical Shift Correlation Spectra of Membrane Proteins by Solid-State MAS NMR Difference Spectroscopy

The feasibility of using difference spectroscopy, i.e. subtraction of two correlation spectra at different mixing times, for substantially enhanced resolution in crowded two-dimensional (13)C-(13)C chemical shift correlation spectra is presented. With the analyses of (13)C-(13)C spin diffusion in si...

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Main Authors: Miao, Yimin, Cross, Timothy A., Fu, Riqiang
Formato: Artigo
Idioma:Inglês
Publicado: 2013
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Acceso en liña:https://ncbi.nlm.nih.gov/pmc/articles/PMC3717563/
https://ncbi.nlm.nih.gov/pubmed/23708936
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-013-9745-7
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