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Two-Step, One-Pot Synthesis of Inosine, Guanosine, and 2′-Deoxyguanosine O(6)-Ethers via Intermediate O(6)-(Benzotriazoly-1-yl) Derivatives
A simple method for the etherification at the O(6)-position of silyl-protected inosine, guanosine, and 2′-deoxyguanosine is described. Typically, a THF solution of the silylated nucleoside is treated with 1H-benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate (BOP) and Cs(2)CO(3)...
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| Auteurs principaux: | , |
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| Format: | Artigo |
| Langue: | Inglês |
| Publié: |
2012
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| Sujets: | |
| Accès en ligne: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3711131/ https://ncbi.nlm.nih.gov/pubmed/22700333 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/0471142700.nc0126s49 |
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