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MODIFIED SYNTHESIS OF 3′-OTBDPS-PROTECTED FURANOID GLYCAL
Thermolytic cleavage of 3′-OH protected thymidine is the most common method of preparing furanoid glycals. We have observed that glycosidic bond cleavage is more facile when the 5′-OH of thymidine was also protected with a silyl group. Addition of trimethylsilyl chloride facilitated cleavage of the...
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| Main Authors: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2012
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3701156/ https://ncbi.nlm.nih.gov/pubmed/22444193 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1080/15257770.2012.656212 |
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