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Influence of deuteration in the glassing matrix on (13)C dynamic nuclear polarization()
Replacement of protons by deuterons in the glassing solvents led to 2–3-fold improvement of the (13)C dynamic nuclear polarization (DNP) solid-state NMR signal for samples doped with large electron spin resonance (ESR) linewidth free radicals galvinoxyl, DPPH, and 4-oxo-TEMPO. Meanwhile, the reverse...
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| Main Authors: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2013
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3681295/ https://ncbi.nlm.nih.gov/pubmed/23552448 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c3cp50750e |
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