High-Field (13)C DNP with a Radical Mixture

We report direct (13)C dynamic nuclear polarization at 5 T under magic angle spinning (MAS) at 82 K using a mixture of monoradicals with narrow EPR linewidths. We show the importance of optimizing both EPR linewidth and electron relaxation times by studying direct DNP of (13)C using SA-BDPA and trit...

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Bibliografiske detaljer
Main Authors: Michaelis, Vladimir K., Smith, Albert A., Corzilius, Björn, Haze, Oleysa, Swager, Timothy M., Griffin, Robert G.
Format: Artigo
Sprog:Inglês
Udgivet: 2013
Fag:
Article
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC3605040/
https://ncbi.nlm.nih.gov/pubmed/23373472
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja312265x
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