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High-Field (13)C DNP with a Radical Mixture
We report direct (13)C dynamic nuclear polarization at 5 T under magic angle spinning (MAS) at 82 K using a mixture of monoradicals with narrow EPR linewidths. We show the importance of optimizing both EPR linewidth and electron relaxation times by studying direct DNP of (13)C using SA-BDPA and trit...
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| Main Authors: | , , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2013
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC3605040/ https://ncbi.nlm.nih.gov/pubmed/23373472 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja312265x |
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