Dynamic Nuclear Polarization of Sedimented Solutes

Using the 480 kDa iron-storage protein complex, apoferritin, as an example, we demonstrate that sizable dynamic nuclear polarization (DNP) enhancements can be obtained on sedimented protein samples. In sedimented solute DNP (SedDNP), the biradical polarizing agent is co-sedimented with the protein,...

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Main Authors: Ravera, Enrico, Corzilius, Björn, Michaelis, Vladimir K., Rosa, Camilla, Griffin, Robert G., Luchinat, Claudio, Bertini, Ivano
Format: Artigo
Sprog:Inglês
Udgivet: 2013
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Article
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC3578289/
https://ncbi.nlm.nih.gov/pubmed/23331059
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja312553b
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