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Accurate Sampling of High-Frequency Motions in Proteins by Steady-State (15)N-{(1)H} Nuclear Overhauser Effect Measurements in the Presence of Cross-Correlated Relaxation

The steady-state {(1)H}-(15)N NOE experiment is used in most common NMR analyses of backbone dynamics to accurately ascertain the effects of the fast dynamic modes. We demonstrate here that, in its most common implementation, this experiment generates an incorrect steady state in the presence of CSA...

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書誌詳細
主要な著者: Ferrage, Fabien, Cowburn, David, Ghose, Ranajeet
フォーマット: Artigo
言語:Inglês
出版事項: 2009
主題:
オンライン・アクセス:https://ncbi.nlm.nih.gov/pmc/articles/PMC3547682/
https://ncbi.nlm.nih.gov/pubmed/19358609
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja809526q
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