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Acid-mediated coupling of γ-hydroxybutenolides and aldehydes: Synthesis of a new class of spirocyclic ketal-lactones

In the presence of trimethylsilyl trifluoromethanesulfonate (TMSOTf), γ-methyl-γ-hydroxybutenolide reacts with aromatic aldehydes to generate a new class of stereochemically rich spirocyclic ketal-lactones in good yields and with excellent stereoselectivities. We believe that this process takes plac...

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Autores principales: Munoz, Alberto, Murelli, Ryan P.
Formato: Artigo
Lenguaje:Inglês
Publicado: 2012
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Acceso en línea:https://ncbi.nlm.nih.gov/pmc/articles/PMC3546829/
https://ncbi.nlm.nih.gov/pubmed/23335822
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2012.09.139
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