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C-Terminal Protein Characterization by Mass Spectrometry using Combined Micro Scale Liquid and Solid-Phase Derivatization

A sample preparation method for protein C-terminal peptide isolation has been developed. In this strategy, protein carboxylate glycinamidation was preceded by carboxyamidomethylation and optional α- and ϵ-amine acetylation in a one-pot reaction, followed by tryptic digestion of the modified protein....

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Detalhes bibliográficos
Main Authors: Nika, Heinz, Nieves, Edward, Hawke, David H., Angeletti, Ruth Hogue
Formato: Artigo
Idioma:Inglês
Publicado em: Association of Biomolecular Resource Facilities 2013
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3518879/
https://ncbi.nlm.nih.gov/pubmed/23543807
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.7171/jbt.13-2401-003
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