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Electron spray ionization mass spectrometry and 2D (31)P NMR for monitoring (18)O/(16)O isotope exchange and turnover rates of metabolic oligophosphates

A new method was here developed for determination of (18)O labeling ratios in metabolic oligophosphates, such as ATP, at different phosphoryl moieties (α-, β-, and γ-ATP) using sensitive and rapid electrospray ionization mass spectrometry (ESI-MS). The ESI-MS based method for monitoring of (18)O/(16...

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Detalhes bibliográficos
Main Authors: Nemutlu, Emirhan, Juranic, Nenad, Zhang, Song, Ward, Lawrence E., Dutta, Tumpa, Nair, K. Sreekumaran, Terzic, Andre, Macura, Slobodan, Dzeja, Petras P.
Formato: Artigo
Idioma:Inglês
Publicado em: 2012
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3349359/
https://ncbi.nlm.nih.gov/pubmed/22427058
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s00216-012-5899-5
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