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Slow Histidine H/D Exchange Protocol for Thermodynamic Analysis of Protein Folding and Stability using Mass Spectrometry

Described here is a mass spectrometry based protocol to study the thermodynamic stability of proteins and protein-ligand complexes using the slow H/D exchange reaction of the imidazole C(2) proton in histidine side chains. The protocol, which involves evaluating the denaturant dependence of this slo...

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Detalhes bibliográficos
Main Authors: Tran, Duc T., Banerjee, Sambuddha, Alayash, Abdu I., Crumbliss, Alvin L., Fitzgerald, Michael C.
Formato: Artigo
Idioma:Inglês
Publicado em: 2012
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3329159/
https://ncbi.nlm.nih.gov/pubmed/22185579
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ac202927p
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