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Asymmetric Synthesis of d-ribo-Phytosphingosine from 1-Tetradecyne and (4-Methoxyphenoxy)acetaldehyde

[Image: see text] An asymmetric synthesis of d-ribo-phytosphingosine (1) was achieved by utilizing the ProPhenol-catalyzed alkynylation of aldehyde 8 to afford allylic propargylic alcohol (S)-6 followed by asymmetric epoxidation and opening of propargylic epoxy alcohol anti-5 with NaN(3)/NH(4)Cl. De...

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Detalhes bibliográficos
Main Authors: Liu, Zheng, Byun, Hoe-Sup, Bittman, Robert
Formato: Artigo
Idioma:Inglês
Publicado em: 2010
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC2892910/
https://ncbi.nlm.nih.gov/pubmed/20527744
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo100707d
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