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HNCO-based measurement of one-bond amide (15)N-(1)H couplings with optimized precision

A pair of 3D HNCO-based experiments have been developed with the aim of optimizing the precision of measurement of (1)J(NH) couplings. Both pulse sequences record (1)J(NH) coupling evolution during the entire constant time interval that (15)N magnetization is dephasing or rephasing with respect to t...

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Detalhes bibliográficos
Main Authors: Arbogast, Luke, Majumdar, Ananya, Tolman, Joel R.
Formato: Artigo
Idioma:Inglês
Publicado em: 2009
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC2827309/
https://ncbi.nlm.nih.gov/pubmed/20012159
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-009-9391-2
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