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Synthesis of 3-(phenylazo)-1,2,4-triazoles by a nucleophilic reaction of primary amines with 5-chloro-2,3-diphenyltetrazolium salt via mesoionic 2,3-diphenyltetrazolium-5-aminides

The reactions of a 5-chloro-2,3-diphenyltetrazolium salt with amines have been examined. In the presence of an inorganic base such as NaHCO(3), primary and secondary amines undergo a nucleophilic substitution to give the corresponding 5-aminotetrazolium salts. When triethylamine is used as a base, p...

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Bibliografiske detaljer
Main Authors: Araki, Shuki, Hirose, Satoshi, Konishi, Yoshikazu, Nogura, Masatoshi, Hirashita, Tsunehisa
Format: Artigo
Sprog:Inglês
Udgivet: Beilstein-Institut 2009
Fag:
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC2686317/
https://ncbi.nlm.nih.gov/pubmed/19478914
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.5.8
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