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Solid-Phase Synthesis of α-Glucosamine Sulfoforms With Fragmentation Analysis by Tandem Mass Spectrometry
Sulfated epitopes of α-glucosamine (GlcN sulfoforms) were prepared by solid-phase synthesis as models of internal glucosamines within heparan sulfate. An orthogonally protected 2’-hydroxyethyl GlcN derivative was immobilized on a trityl resin support and subjected to regioselective deprotection and...
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| Hlavní autoři: | , , , , , , |
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| Médium: | Artigo |
| Jazyk: | Inglês |
| Vydáno: |
2008
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| Témata: | |
| On-line přístup: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2613357/ https://ncbi.nlm.nih.gov/pubmed/18610984 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo800713m |
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