Solid-Phase Synthesis of α-Glucosamine Sulfoforms With Fragmentation Analysis by Tandem Mass Spectrometry

Sulfated epitopes of α-glucosamine (GlcN sulfoforms) were prepared by solid-phase synthesis as models of internal glucosamines within heparan sulfate. An orthogonally protected 2’-hydroxyethyl GlcN derivative was immobilized on a trityl resin support and subjected to regioselective deprotection and...

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Библиографические подробности
Главные авторы: Liu, Runhui, Chanthamontri, Chamnongsak, Han, Hongling, Hernández-Torres, Jesús M., Wood, Karl V., McLuckey, Scott A., Wei, Alexander
Формат: Artigo
Язык:Inglês
Опубликовано: 2008
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Article
Online-ссылка:https://ncbi.nlm.nih.gov/pmc/articles/PMC2613357/
https://ncbi.nlm.nih.gov/pubmed/18610984
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo800713m
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