Stable Isotope-Coded Quaternization for Comparative Quantification of Estrogen Metabolites by High-Performance Liquid Chromatography-Electrospray Ionization Mass Spectrometry

A fast and sensitive LC-ESI-MS method is described for the comparative quantification of 16 estrogen metabolites based on the derivatization of estrogens with a novel derivatizing reagent, N-methyl-nicotinic acid N-hydroxysuccinimide ester (C1-NA-NHS). The process introduces a quaternary amine to th...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: Yang, Wen-Chu, Regnier, Fred E., Sliva, Dan, Adamec, Jiri
Format: Artigo
Sprache:Inglês
Veröffentlicht: 2008
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Article
Online Zugang:https://ncbi.nlm.nih.gov/pmc/articles/PMC2572562/
https://ncbi.nlm.nih.gov/pubmed/18595786
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jchromb.2008.06.026
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