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Characterization of oxysterols by electrospray ionization tandem mass spectrometry after one-step derivatization with dimethylglycine
We report a novel approach to derivatize the primary, secondary, and tertiary hydroxy group(s) of oxysterols with N,N-dimethylglycine (DMG) in the presence of both 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide and 4-(N,N-dimethylamino)pyridine to yield their corresponding mono- or di-DMG esters. Eig...
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| Main Authors: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2007
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2151840/ https://ncbi.nlm.nih.gov/pubmed/17154356 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/rcm.2820 |
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