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Differentiation of chiral phosphorus enantiomers by (31)P and (1)H NMR spectroscopy using amino acid derivatives as chemical solvating agents
The ability of commercially available amino acid derivatives, especially Fmoc-Trp(Boc)-OH, to differentiate enantiomers of chiral phosphonates, phosphinates, phosphates, phosphine oxides, and phosphonamidates is demonstrated with (31)P, (13)C, and (1)H NMR spectroscopy. The chiral differentiation pr...
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| Main Authors: | , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2007
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2084221/ https://ncbi.nlm.nih.gov/pubmed/18037983 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetasy.2007.06.012 |
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