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Solid-Phase Synthesis and Configurational Reassigment of Callipeltin E. Implications for the Structures of Callipeltins A and B.
[Figure: see text] Two possible isomers of the natural product callipeltin E (1, 5), were synthesized using an Fmoc-based solid-phase strategy in 7 steps, in 20% and 26% overall yields, respectively. The (1)H-NMR spectrum of synthetic 5 correlated closely with that of the natural product, whereas th...
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| Main Authors: | , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2006
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC1584402/ https://ncbi.nlm.nih.gov/pubmed/16901115 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo060351h |
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