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Determination of residual solvents in synthetic intermediate of Selexipag by headspace gas chromatograhy

In order to better control the quality of Selexipag products and ensure drug safety,headspace gas chromatography is established to detect the amount of solvent remaining in the synthesis of Selexipag intermediates 4-\ pyrazin -2-yl) (isopropyl) amino\]-1-butanol (S5) and N-(2-chloroacetyl) methyl su...

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Principais autores: Haijuan QI, Haoliang CUI, Xiaoqing DENG, Hongpeng WANG, Shuangshuang GAO, Jing HA
Format: Artigo
Sprog:Chinês
Udgivet: Hebei University of Science and Technology 2019-06-01
Serier:Journal of Hebei University of Science and Technology
Fag:
chromatographic analysis
headspace gas chromatography
residual solvent
Selexipag
intermediate
content determination
Online adgang:http://xuebao.hebust.edu.cn/hbkjdx/ch/reader/create_pdf.aspx?file_no=b201903005&flag=1&journal_
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