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NMR and Computational Studies as Analytical and High-Resolution Structural Tool for Complex Hydroperoxides and Diastereomeric <i>Endo</i>-Hydroperoxides of Fatty Acids in Solution-Exemplified by Methyl Linolenate

A combination of selective 1D Total Correlation Spectroscopy (TOCSY) and <sup>1</sup>H-<sup>13</sup>C Heteronuclear Multiple Bond Correlation (HMBC) NMR techniques has been employed for the identification of methyl linolenate primary oxidation products without the need for laborious isolation of the...

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Principais autores: Raheel Ahmed, Panayiotis C. Varras, Michael G. Siskos, Hina Siddiqui, M. Iqbal Choudhary, Ioannis P. Gerothanassis
Format: Artigo
Sprog:Inglês
Udgivet: MDPI AG 2020-10-01
Serier:Molecules
Fag:
polyunsaturated fatty acids
hydroperoxides
<i>endo</i>-hydroperoxides
NMR
chemical shifts
hydrogen bonding
Online adgang:https://www.mdpi.com/1420-3049/25/21/4902
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