On the Use of Deuterated Organic Solvents without TMS to Report ¹H/¹³C NMR Spectral Data of Organic Compounds: Current State of the Method, Its Pitfalls and Benefits, and Related Issues

The quite popular, simple but imperfect method of referencing NMR spectra to residual ¹H and ¹³C signals of TMS-free deuterated organic solvents (referred to as Method A) is critically discussed for six commonly used NMR solvents with respect to their δ_H and δ<sub>C<...

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Autore principale:	Ryszard B. Nazarski
Natura:	Artigo
Lingua:	Inglês
Pubblicazione:	MDPI AG 2023-05-01
Serie:	Molecules
Soggetti:	NMR spectroscopy tetramethylsilane internal reference standards deuterated solvent signals residual <sup>1</sup>H signals the IUPAC unified <i>Ξ</i> scale of chemical shifts
Accesso online:	https://www.mdpi.com/1420-3049/28/11/4369
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