On the Use of Deuterated Organic Solvents without TMS to Report ¹H/¹³C NMR Spectral Data of Organic Compounds: Current State of the Method, Its Pitfalls and Benefits, and Related Issues

The quite popular, simple but imperfect method of referencing NMR spectra to residual ¹H and ¹³C signals of TMS-free deuterated organic solvents (referred to as Method A) is critically discussed for six commonly used NMR solvents with respect to their δ_H and δ<sub>C<...

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Bibliografski detalji

Glavni autor:	Ryszard B. Nazarski
Format:	Artigo
Jezik:	Inglês
Izdano:	MDPI AG 2023-05-01
Serija:	Molecules
Teme:	NMR spectroscopy tetramethylsilane internal reference standards deuterated solvent signals residual <sup>1</sup>H signals the IUPAC unified <i>Ξ</i> scale of chemical shifts
Online pristup:	https://www.mdpi.com/1420-3049/28/11/4369
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