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Cyclization of interlocked fumaramides into β-lactams: experimental and computational mechanistic assessment of the key intercomponent proton transfer and the stereocontrolling active pocket

A detailed mechanistic study of the diastereoselective CsOH-promoted cyclization of interlocked fumaramides to give β-lactams is described. The mechanistic analysis comprises the experimental evaluation of the structure-reactivity relationship for a wide range of fumaramides [2]rotaxanes (Hammet-plo...

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Vydáno v:Chem Sci
Hlavní autoři: Martinez-Cuezva, Alberto, Pastor, Aurelia, Marin-Luna, Marta, Diaz-Marin, Carmen, Bautista, Delia, Alajarin, Mateo, Berna, Jose
Médium: Artigo
Jazyk:Inglês
Vydáno: The Royal Society of Chemistry 2020
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On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC8178992/
https://ncbi.nlm.nih.gov/pubmed/34163808
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/d0sc05757f
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