Conventional vs. Microwave- or Mechanically-Assisted Synthesis of Dihomooxacalix[4]arene Phthalimides: NMR, X-ray and Photophysical Analysis (§)

Direct O-alkylation of p-tert-butyldihomooxacalix[4]arene (1) with N-(bromopropyl)- or N-(bromoethyl)phthalimides and K(2)CO(3) in acetonitrile was conducted under conventional heating (reflux) and using microwave irradiation and ball milling methodologies. The reactions afforded mono- and mainly di...

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Publicado en:Molecules
Autores principales: Miranda, Alexandre S., Marcos, Paula M., Ascenso, José R., Robalo, M. Paula, Bonifácio, Vasco D. B., Berberan-Santos, Mário N., Hickey, Neal, Geremia, Silvano
Formato: Artigo
Lenguaje:Inglês
Publicado: MDPI 2021
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Article
Acceso en línea:https://ncbi.nlm.nih.gov/pmc/articles/PMC7998390/
https://ncbi.nlm.nih.gov/pubmed/33801929
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3390/molecules26061503
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