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Optimisation of Urine Sample Preparation for Headspace-Solid Phase Microextraction Gas Chromatography-Mass Spectrometry: Altering Sample pH, Sulphuric Acid Concentration and Phase Ratio

Headspace-solid phase microextraction gas chromatography-mass spectrometry (HS-SPME-GC-MS) can be used to measure volatile organic compounds (VOCs) in human urine. However, there is no widely adopted standardised protocol for the preparation of urine samples for analysis resulting in an inability to...

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Detalhes bibliográficos
Publicado no:Metabolites
Main Authors: Aggarwal, Prashant, Baker, James, Boyd, Mark T., Coyle, Séamus, Probert, Chris, Chapman, Elinor A.
Formato: Artigo
Idioma:Inglês
Publicado em: MDPI 2020
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC7760603/
https://ncbi.nlm.nih.gov/pubmed/33255680
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3390/metabo10120482
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