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Catalytic enantioselective synthesis of carbocyclic and heterocyclic spiranes via a decarboxylative aldol cyclization

The synthesis of a variety of enantioenriched 1,3-diketospiranes from the corresponding racemic allyl β-ketoesters via an interrupted asymmetric allylic alkylation is disclosed. Substrates possessing pendant aldehydes undergo decarboxylative enolate formation in the presence of a chiral Pd catalyst...

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Detalhes bibliográficos
Publicado no:Chem Sci
Main Authors: Inanaga, Kazato, Wollenburg, Marco, Bachman, Shoshana, Hafeman, Nicholas J., Stoltz, Brian M.
Formato: Artigo
Idioma:Inglês
Publicado em: Royal Society of Chemistry 2020
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC7574022/
https://ncbi.nlm.nih.gov/pubmed/33133488
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/d0sc02366c
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