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Building up Strain in One Step: Synthesis of an Edge‐Fused Double Silacyclobutene from an Extensively Trichlorosilylated Butadiene Dianion
The exhaustive trichlorosilylation of hexachloro‐1,3‐butadiene was achieved in one step by using a mixture of Si(2)Cl(6) and [nBu(4)N]Cl (7:2 equiv) as the silylation reagent. The corresponding butadiene dianion salt [nBu(4)N](2)[1] was isolated in 36 % yield after recrystallization. The negative ch...
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| Publicado no: | Angew Chem Int Ed Engl |
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| Main Authors: | , , , , , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
John Wiley and Sons Inc.
2020
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC7540532/ https://ncbi.nlm.nih.gov/pubmed/32484309 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.202006463 |
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