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Gram-scale preparation of the antibiotic lead compound salicyl-AMS, a potent inhibitor of bacterial salicylate adenylation enzymes

Salicyl-AMS (1) is a potent inhibitor of salicylate adenylation enzymes used in bacterial siderophore biosynthesis and a promising lead compound for the treatment of tuberculosis. An optimized, multigram synthesis is presented, which provides salicyl-AMS as its sodium salt (1·Na) in three synthetic...

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Publicat a:Methods Enzymol
Autors principals: Kinarivala, Nihar, Standke, Lisa C., Guney, Tezcan, Ji, Cheng, Noguchi, Naoyoshi, Asano, Yasutomi, Tan, Derek S.
Format: Artigo
Idioma:Inglês
Publicat: 2020
Matèries:
Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC7367610/
https://ncbi.nlm.nih.gov/pubmed/32416922
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/bs.mie.2020.04.051
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