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Practical Synthesis of Ethynyl(phenyl)-λ(3)-Iodane Using Calcium Carbide as an Ethynyl Group Source
Stannylation of calcium carbide followed by Sn–hypervalent iodine(III) exchange reaction cleanly afforded the electrophilic ethynylating agent ethynyl(phenyl)-λ(3)-iodane in high yield. This two-step method uses very inexpensive materials and is readily operable without any special precautions.
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| Publicat a: | Front Chem |
|---|---|
| Autors principals: | , , , |
| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
Frontiers Media S.A.
2020
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC7010717/ https://ncbi.nlm.nih.gov/pubmed/32117863 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3389/fchem.2020.00012 |
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