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An aqueous normal-phase chromatography coupled with tandem mass spectrometry method for determining unbound brain-to-plasma concentration ratio of AZD1775, a Wee1 kinase inhibitor, in patients with glioblastoma

A rapid, sensitive, and robust aqueous normal-phase chromatography method coupled with tandem mass spectrometry was developed and validated for the quantitation of AZD1775, a Wee-1 inhibitor, in human plasma and brain tumor tissue. Sample preparation involved simple protein precipitation with aceton...

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Bibliografske podrobnosti
izdano v:J Chromatogr B Analyt Technol Biomed Life Sci
Main Authors: Wu, Jianmei, Sanai, Nader, Bao, Xun, LoRusso, Patricia, Li, Jing
Format: Artigo
Jezik:Inglês
Izdano: 2016
Teme:
Online dostop:https://ncbi.nlm.nih.gov/pmc/articles/PMC6863148/
https://ncbi.nlm.nih.gov/pubmed/27318641
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.jchromb.2016.05.050
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