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An Improved Procedure for Synthesis of DL-4-Hydroxy-3-methoxymandelic Acid (DL-“Vanillyl”-mandelic Acid, VMA)

An improved procedure for synthesis of DL-4-Hydroxy-3-methoxymandelic Acid (DL-Vanillyl-mandelic Acid, VMA) entails slow addition of an ice-cold, aqueous solution of glyoxylic acid to an ice-cold alkaline solution of guaiacol, with efficient mechanical stirring. This one-step condensation procedure...

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Detalhes bibliográficos
Publicado no:J Res Natl Bur Stand A Phys Chem
Main Authors: Fatiadi, Alexander J., Schaffer, Robert
Formato: Artigo
Idioma:Inglês
Publicado em: National Institute of Standards and Technology 1974
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC6742820/
https://ncbi.nlm.nih.gov/pubmed/32189791
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.6028/jres.078A.024
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