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An Improved Procedure for Synthesis of DL-4-Hydroxy-3-methoxymandelic Acid (DL-“Vanillyl”-mandelic Acid, VMA)
An improved procedure for synthesis of DL-4-Hydroxy-3-methoxymandelic Acid (DL-Vanillyl-mandelic Acid, VMA) entails slow addition of an ice-cold, aqueous solution of glyoxylic acid to an ice-cold alkaline solution of guaiacol, with efficient mechanical stirring. This one-step condensation procedure...
Guardat en:
| Publicat a: | J Res Natl Bur Stand A Phys Chem |
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| Autors principals: | , |
| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
National Institute of Standards and Technology
1974
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6742820/ https://ncbi.nlm.nih.gov/pubmed/32189791 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.6028/jres.078A.024 |
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