Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction

Using time‐resolved monochromatic high energy X‐ray diffraction, we present an in situ study of the solvothermal crystallisation of a new MOF [Yb(2)(BDC)(3)(DMF)(2)]⋅H(2)O (BDC=benzene‐1,4‐dicarboxylate and DMF=N,N‐dimethylformamide) under solvothermal conditions, from mixed water/DMF solvent. Analy...

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Detalhes bibliográficos
Publicado no:Angew Chem Int Ed Engl
Main Authors: Wu, Yue, Breeze, Matthew I., Clarkson, Guy J., Millange, Franck, O'Hare, Dermot, Walton, Richard I.
Formato: Artigo
Idioma:Inglês
Publicado em: John Wiley and Sons Inc. 2016
Assuntos:
Communications
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC6680260/
https://ncbi.nlm.nih.gov/pubmed/26959076
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201600896
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