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UO(2)(2+)-mediated ring contraction of pyrihexaphyrin: synthesis of a contracted expanded porphyrin-uranyl complex

A new mixed hexaphyrin, pyrihexaphyrin (0.1.0.0.1.0) (1), was prepared via an acid catalyzed cyclization between 5,5′-(pyridine-2,6-diyl)bis(pyrrole-2-carbaldehyde) (2) and terpyrrole (3). This expanded porphyrin undergoes a ring contraction upon metallation with uranyl silylamide [UO(2)[N(SiMe(3))(...

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Publicat a:Chem Sci
Autors principals: Brewster, James T., Root, Harrison D., Mangel, Daniel, Samia, Adam, Zafar, Hadiqa, Sedgwick, Adam C., Lynch, Vincent M., Sessler, Jonathan L.
Format: Artigo
Idioma:Inglês
Publicat: Royal Society of Chemistry 2019
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Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC6552508/
https://ncbi.nlm.nih.gov/pubmed/31293744
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/c9sc01593k
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