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Ultra-high Resolution Band-Selective HSQC for Nanomole-Scale Identification of Chlorine-Substituted (13)C in Natural Products Drug Discovery
Ultra-high resolution band-selective HSQC (bsHSQC) has been employed for detection of (35)Cl-(37)Cl isotope shifted (13)C NMR signals for assignment of regioisomerism in bromo-chloro natural products. Optimum pulse sequence and instrumental parameters for maximization of detection of the isotope shi...
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| Publicado no: | Magn Reson Chem |
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| Main Authors: | , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6411301/ https://ncbi.nlm.nih.gov/pubmed/26951950 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/mrc.4415 |
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