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Synthesis of Perfluoro-tert-butyl Tyrosine, for Application in (19)F NMR, via a Diazonium Coupling Reaction
A practical synthesis of the novel highly fluorinated amino acid Fmoc-perfluoro-tert-butyl tyrosine was developed. The sequence proceeds in 2 steps from commercially available Fmoc-4-NH(2)-phenylalanine, via diazotization followed by diazonium coupling reaction with perfluoro-tert-butanol. In peptid...
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| Publicado no: | Org Lett |
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| Main Authors: | , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6354588/ https://ncbi.nlm.nih.gov/pubmed/27978684 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.orglett.6b02858 |
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