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In Situ Investigation of a Self-Accelerated Cocrystal Formation by Grinding Pyrazinamide with Oxalic Acid

A new cocrystal of pyrazinamide with oxalic acid was prepared mechanochemically and characterized by PXRD, Raman spectroscopy, solid-state NMR spectroscopy, DTA-TG, and SEM. Based on powder X-ray diffraction data the structure was solved. The formation pathway of the reaction was studied in situ usi...

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Bibliographische Detailangaben
Veröffentlicht in:Molecules
Hauptverfasser: Kulla, Hannes, Greiser, Sebastian, Benemann, Sigrid, Rademann, Klaus, Emmerling, Franziska
Format: Artigo
Sprache:Inglês
Veröffentlicht: MDPI 2016
Schlagworte:
Online Zugang:https://ncbi.nlm.nih.gov/pmc/articles/PMC6274108/
https://ncbi.nlm.nih.gov/pubmed/27428942
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3390/molecules21070917
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