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The first spontaneous resolution of a sulfoxide: Dianin’s compound analogue, (R)-4-(4-hydroxyphenyl)-2,2,4-trimethylthiachroman-1-oxide
The title sulfoxide, C(18)H(20)O(2)S, was prepared by controlled oxidation of thia-Dianin’s compound using hydrogen peroxide in glacial acetic acid. On recrystallization from glacial acetic acid, it was found to form unsolvated, spontaneously resolved crystals, the initial crystal structure analysis...
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| Publicado no: | Acta Crystallogr E Crystallogr Commun |
|---|---|
| Main Authors: | , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
International Union of Crystallography
2018
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6218920/ https://ncbi.nlm.nih.gov/pubmed/30443396 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1107/S2056989018014366 |
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