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Direct Photochemical C–H Carboxylation of Aromatic Diamines with CO(2) under Electron-Donor- and Base-free Conditions
We report the photochemical carboxylation of o-phenylenedimamine in the absence of a base and an electron donor under an atmosphere of CO(2), which afforded 2,3-diaminobenzoic acid (DBA) in 28% synthetic yield and 0.22% quantum yield (Φ(%)). The synthetic yield of DBA in this reaction increased to 5...
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| Publicado no: | Sci Rep |
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| Main Authors: | , , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
Nature Publishing Group UK
2018
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6168591/ https://ncbi.nlm.nih.gov/pubmed/30279606 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1038/s41598-018-33060-3 |
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